郑修成,袁程远,赵文平,杨春艳,叶文豪,王向宇

• 1:郑州大学化学系
• 2:郑州大学化学系
• 3:郑州大学化学系
• 4:郑州大学化学系

摘要(Abstract)：

以三嵌段共聚物P123为模板剂、正硅酸乙酯为硅源,水热合成了介孔分子筛SBA-15,利用N2吸附-脱附、XRD、TEM等手段对其进行了表征,并考察了SiO2/P123摩尔比、反应溶液酸度、共溶剂等因素对其结构的影响.结果表明,随着SiO2/P123摩尔比的增加,介孔分子筛SBA-15的比表面无显著变化,孔径、孔容逐渐减小;随着反应溶液酸度的增强,样品比表面无明显变化,而孔径、孔容则明显变大;不同共溶剂的扩容效果不一,其中三甲苯的效果最佳.

关键词(KeyWords)： 水热合成;介孔分子筛SBA-15;酸度;共溶剂

Abstract:

Keywords:

基金项目(Foundation): 河南省杰出人才创新基金,编号0221001200;; 郑州大学引进人才专项基金

作者(Author): 郑修成,袁程远,赵文平,杨春艳,叶文豪,王向宇

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